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1 article(s) from Manley, David W

Preparative semiconductor photoredox catalysis: An emerging theme in organic synthesis

David W. Manley and
John C. Walton

Beilstein J. Org. Chem. 2015, 11, 1570–1582, doi:10.3762/bjoc.11.173

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Graphical Abstract

Figure 1: Production and utilization of h⁺ and e^– by photoactivation of a semiconductor.

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Figure 2: Photoredox activity of TiO₂ with moist air.

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Scheme 1: TiO₂ promoted oxidation of phenanthrene [29].

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Scheme 2: SCPC assisted additions of allylic compounds to diazines and imines [40-42].

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Scheme 3: TiO₂ promoted addition and addition–cyclization reactions of tert-amines with electron-deficient al...

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Scheme 4: Reactions of amines promoted by Pt-TiO₂ [48,49].

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Scheme 5: P25 Promoted alkylations of N-phenylmaleimide with diverse carboxylic acids [53,54]. ^aAccompanied by R–R d...

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Scheme 6: SCPC cyclizations of aryloxyacetic acids with suitably sited alkene acceptors [54]. ^aYields in brackets...

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Scheme 7: TiO₂ promoted reactions of aryloxyacetic acids with maleic anhydride and maleimides [53,54].

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Scheme 8: Photoredox addition–cyclization reactions of aryloxyacetic and related acids promoted by maleimide [63]....

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Scheme 9: SCPC promoted homo-couplings and macrocyclizations with carboxylic acids [64].

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Scheme 10: TiO₂ promoted alkylations of alkenes with silanes [66] and thiols [67].

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Scheme 11: TiO₂ reduction of a nitrochromenone derivative [70].

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Scheme 12: TiO₂ mediated hydrodehalogenations and cyclizations of organic iodides [71].

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Scheme 13: TiO₂ promoted hydrogenations of maleimides, maleic anhydride and aromatic aldehydes [79].

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Scheme 14: Mechanistic sketch of SCPC hydrogenation of aryl aldehydes.

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Review

Published 09 Sep 2015

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